Crystallography Open Database

Information card for entry 7711771

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Coordinates	7711771.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C109 H146 Cl12 N12 W3
Calculated formula	C109 H146 Cl12 N12 W3
Title of publication	N Heterocyclic Carbene and Cyclic (Alkyl)(amino)carbene Complexes of Molybdenum(IV) and Tungsten(IV)
Authors of publication	Luz, Christian; Glok, Eduard; Horrer, Günther; Radius, Udo
Journal of publication	Dalton Transactions
Year of publication	2022
a	20.5525 ± 0.0001 Å
b	25.8044 ± 0.0002 Å
c	25.933 ± 0.0002 Å
α	114.543 ± 0.001°
β	105.947 ± 0.001°
γ	94.478 ± 0.001°
Cell volume	11735.3 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0411
Residual factor for significantly intense reflections	0.0349
Weighted residual factors for significantly intense reflections	0.084
Weighted residual factors for all reflections included in the refinement	0.0868
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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