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Information card for entry 7711932
Preview
Coordinates | 7711932.cif |
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Original paper (by DOI) | HTML |
Chemical name | [{κP,κC-(i-Pr)2PO-(5-Cl-C6H3)}{κN-(PhCH2-)(PhCH=)N}Ni(Br)] |
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Formula | C26 H30 Br Cl N Ni O P |
Calculated formula | C26 H30 Br Cl N Ni O P |
SMILES | Br[Ni]1([P](Oc2c1ccc(Cl)c2)(C(C)C)C(C)C)[N](=Cc1ccccc1)Cc1ccccc1 |
Title of publication | Reactivities of cyclonickellated complexes with hydroxylamines: formation of κ<sup>O</sup>-hydroxylamine and κ<sup>N</sup>-imine adducts and a κ<sup>O</sup>, κ<sup>N</sup>-aminoxide derivative. |
Authors of publication | Sarker, Rajib K.; Mangin, Loïc P; Zargarian, Davit |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
Journal volume | 52 |
Journal issue | 2 |
Pages of publication | 366 - 375 |
a | 12.9011 ± 0.0005 Å |
b | 15.7826 ± 0.0006 Å |
c | 13.2566 ± 0.0005 Å |
α | 90° |
β | 107.169 ± 0.002° |
γ | 90° |
Cell volume | 2578.93 ± 0.17 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0518 |
Residual factor for significantly intense reflections | 0.0374 |
Weighted residual factors for significantly intense reflections | 0.0868 |
Weighted residual factors for all reflections included in the refinement | 0.0935 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation wavelength | 1.34139 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7711932.html
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