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Information card for entry 7711933
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Coordinates | 7711933.cif |
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Original paper (by DOI) | HTML |
Chemical name | [{κP,κC-(i-Pr)2PO-C6H4}{NH2OBn}Ni(Cl/Br)] |
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Formula | C19 H27 Br0.26 Cl0.74 N Ni O2 P |
Calculated formula | C19 H27 Br0.2655 Cl0.7345 N Ni O2 P |
Title of publication | Reactivities of cyclonickellated complexes with hydroxylamines: formation of κ<sup>O</sup>-hydroxylamine and κ<sup>N</sup>-imine adducts and a κ<sup>O</sup>, κ<sup>N</sup>-aminoxide derivative. |
Authors of publication | Sarker, Rajib K.; Mangin, Loïc P; Zargarian, Davit |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
Journal volume | 52 |
Journal issue | 2 |
Pages of publication | 366 - 375 |
a | 9.2167 ± 0.0003 Å |
b | 10.7893 ± 0.0003 Å |
c | 11.1469 ± 0.0003 Å |
α | 108.309 ± 0.001° |
β | 99.259 ± 0.001° |
γ | 99.244 ± 0.001° |
Cell volume | 1011.92 ± 0.05 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0237 |
Residual factor for significantly intense reflections | 0.0236 |
Weighted residual factors for significantly intense reflections | 0.0639 |
Weighted residual factors for all reflections included in the refinement | 0.064 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7711933.html
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