Information card for entry 7712133

Structure parameters

• Formula: C39 H33 Cl4 N2 P2 Rh S
• Calculated formula: C39 H33 Cl4 N2 P2 Rh S
• Title of publication: C-H activation in bimetallic rhodium complexes to afford N-heterocyclic carbene pincer complexes.
• Authors of publication: Watson, Lachlan J.; Hill, Anthony F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 52
• Journal issue: 7
• Pages of publication: 2164 - 2174
• a: 12.1459 ± 0.0006 Å
• b: 12.7759 ± 0.0008 Å
• c: 13.1675 ± 0.0007 Å
• α: 70.396 ± 0.005°
• β: 77.844 ± 0.004°
• γ: 84.928 ± 0.004°
• Cell volume: 1881.32 ± 0.19 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0641
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1294
• Weighted residual factors for all reflections included in the refinement: 0.1418
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No