Information card for entry 7712134

Structure parameters

• Formula: C44 H36 F6 N2 O P3 Rh
• Calculated formula: C44 H36 F6 N2 O P3 Rh
• Title of publication: C-H activation in bimetallic rhodium complexes to afford N-heterocyclic carbene pincer complexes.
• Authors of publication: Watson, Lachlan J.; Hill, Anthony F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 52
• Journal issue: 7
• Pages of publication: 2164 - 2174
• a: 15.2904 ± 0.0003 Å
• b: 16.1205 ± 0.0005 Å
• c: 19.0392 ± 0.0006 Å
• α: 90°
• β: 105.181 ± 0.003°
• γ: 90°
• Cell volume: 4529.2 ± 0.2 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.074
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1048
• Weighted residual factors for all reflections included in the refinement: 0.1163
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No