Information card for entry 7712716

Structure parameters

• Formula: C103 H99.85 Ag0.58 Al Cl0.58 F36 O8.42 P2 Rh
• Calculated formula: C103 H99.8446 Ag0.5777 Al Cl0.5777 F36 O8.4223 P2 Rh
• Title of publication: Template synthesis of an intermediate in silver salt metathesis using a calix[4]arene-based diphosphine ligand
• Authors of publication: Emerson-King, Jack; Chaplin, Adrian B.
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 15.5392 ± 0.0003 Å
• b: 18.958 ± 0.0006 Å
• c: 20.2764 ± 0.0006 Å
• α: 69.264 ± 0.003°
• β: 81.839 ± 0.002°
• γ: 69.584 ± 0.002°
• Cell volume: 5234.3 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1158
• Residual factor for significantly intense reflections: 0.0771
• Weighted residual factors for significantly intense reflections: 0.1933
• Weighted residual factors for all reflections included in the refinement: 0.2199
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No