Information card for entry 7712717

Structure parameters

• Formula: C159 H163 Cl2 O8 P4 Rh2
• Calculated formula: C159 H163 Cl2 O8 P4 Rh2
• Title of publication: Template synthesis of an intermediate in silver salt metathesis using a calix[4]arene-based diphosphine ligand
• Authors of publication: Emerson-King, Jack; Chaplin, Adrian B.
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 17.9994 ± 0.0008 Å
• b: 18.5281 ± 0.0008 Å
• c: 21.3105 ± 0.0014 Å
• α: 75.02 ± 0.005°
• β: 87.021 ± 0.004°
• γ: 89.684 ± 0.004°
• Cell volume: 6855.9 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1793
• Residual factor for significantly intense reflections: 0.1471
• Weighted residual factors for significantly intense reflections: 0.3643
• Weighted residual factors for all reflections included in the refinement: 0.3859
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No