Information card for entry 7712775

Structure parameters

• Formula: C30 H30 Cl2 O2 P2 Pd
• Calculated formula: C30 H30 Cl2 O2 P2 Pd
• Title of publication: Metal phosphine aldehyde complexes and their application in Cu-free Sonogashira and Suzuki-Miyaura cross-coupling reactions
• Authors of publication: Baweja, Saral; Gabler, Tom; Lönnecke, Peter; Hey-Hawkins, Evamarie
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 7.3786 ± 0.0003 Å
• b: 10.1292 ± 0.0002 Å
• c: 10.4543 ± 0.0003 Å
• α: 104.828 ± 0.002°
• β: 104.879 ± 0.003°
• γ: 96.825 ± 0.002°
• Cell volume: 715.62 ± 0.04 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0291
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0586
• Weighted residual factors for all reflections included in the refinement: 0.0605
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No