Information card for entry 7712774

Structure parameters

• Formula: C30 H30 Cl4 O2 P2 Pd2
• Calculated formula: C30 H30 Cl4 O2 P2 Pd2
• Title of publication: Metal phosphine aldehyde complexes and their application in Cu-free Sonogashira and Suzuki-Miyaura cross-coupling reactions
• Authors of publication: Baweja, Saral; Gabler, Tom; Lönnecke, Peter; Hey-Hawkins, Evamarie
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 7.3184 ± 0.0001 Å
• b: 12.255 ± 0.0002 Å
• c: 17.6833 ± 0.0003 Å
• α: 90°
• β: 90.789 ± 0.001°
• γ: 90°
• Cell volume: 1585.81 ± 0.04 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0795
• Weighted residual factors for all reflections included in the refinement: 0.0854
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No