Information card for entry 7713293

Structure parameters

• Chemical name: Triscarborane_trimehtylphosphine_triethylsilane
• Formula: C15 H58 B31 P Si
• Calculated formula: C15 H58 B31 P Si
• Title of publication: Examining the reactivity of tris(<i>ortho</i>-carboranyl)borane with Lewis bases and application in frustrated Lewis pair Si-H bond cleavage.
• Authors of publication: Vashisth, Kanika; Dutta, Sanjay; Akram, Manjur O.; Martin, Caleb D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• a: 13.0069 ± 0.0003 Å
• b: 13.0069 ± 0.0003 Å
• c: 25.8322 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3784.77 ± 0.17 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 165
• Hermann-Mauguin space group symbol: P -3 c 1
• Hall space group symbol: -P 3 2"c
• Residual factor for all reflections: 0.0752
• Residual factor for significantly intense reflections: 0.055
• Weighted residual factors for significantly intense reflections: 0.1373
• Weighted residual factors for all reflections included in the refinement: 0.1666
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No