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Information card for entry 7713294
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Coordinates | 7713294.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | tris-carborane_triphenylphosphine_triethylsilane |
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Formula | C30 H64 B31 P Si |
Calculated formula | C30 H64 B31 P Si |
Title of publication | Examining the reactivity of tris(<i>ortho</i>-carboranyl)borane with Lewis bases and application in frustrated Lewis pair Si-H bond cleavage. |
Authors of publication | Vashisth, Kanika; Dutta, Sanjay; Akram, Manjur O.; Martin, Caleb D. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
a | 15.5559 ± 0.0007 Å |
b | 15.5559 ± 0.0007 Å |
c | 36.209 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 7588.2 ± 0.8 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 5 |
Space group number | 148 |
Hermann-Mauguin space group symbol | R -3 :H |
Hall space group symbol | -R 3 |
Residual factor for all reflections | 0.0815 |
Residual factor for significantly intense reflections | 0.0677 |
Weighted residual factors for significantly intense reflections | 0.1691 |
Weighted residual factors for all reflections included in the refinement | 0.1802 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.116 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7713294.html
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structural data.