Information card for entry 7715314

Structure parameters

• Formula: C56 H84 K2 O4 P2 Se2
• Calculated formula: C56 H84 K2 O4 P2 Se2
• Title of publication: Coordination chemistry of alkali metal dimesityl-thio- and dimesityl-selenophosphinites [(L)₂A-EPMes₂]₂ (A = Li, Na, K; E = S, Se; L = THF, THP) and [(18C6)K-SPMes₂].
• Authors of publication: Dorow, Richard C. C.; Liebing, Phil; Görls, Helmar; Westerhausen, Matthias
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 12
• Pages of publication: 5711 - 5720
• a: 12.344 ± 0.003 Å
• b: 17.315 ± 0.004 Å
• c: 13.494 ± 0.004 Å
• α: 90°
• β: 92.518 ± 0.01°
• γ: 90°
• Cell volume: 2881.4 ± 1.3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0517
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0701
• Weighted residual factors for all reflections included in the refinement: 0.08
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No