Information card for entry 7715315

Structure parameters

• Formula: C56 H84 K2 O4 P2 S2
• Calculated formula: C56 H84 K2 O4 P2 S2
• Title of publication: Coordination chemistry of alkali metal dimesityl-thio- and dimesityl-selenophosphinites [(L)₂A-EPMes₂]₂ (A = Li, Na, K; E = S, Se; L = THF, THP) and [(18C6)K-SPMes₂].
• Authors of publication: Dorow, Richard C. C.; Liebing, Phil; Görls, Helmar; Westerhausen, Matthias
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 12
• Pages of publication: 5711 - 5720
• a: 13.439 ± 0.0015 Å
• b: 13.7423 ± 0.0014 Å
• c: 17.2067 ± 0.0019 Å
• α: 92.241 ± 0.003°
• β: 108.058 ± 0.003°
• γ: 108.624 ± 0.003°
• Cell volume: 2829.2 ± 0.5 ų
• Cell temperature: 117 ± 2 K
• Ambient diffraction temperature: 117 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1413
• Residual factor for significantly intense reflections: 0.0741
• Weighted residual factors for significantly intense reflections: 0.1568
• Weighted residual factors for all reflections included in the refinement: 0.1974
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No