Information card for entry 7716221

Structure parameters

• Formula: C88 H108 D12 N6 Si5
• Calculated formula: C88 H108 D12 N6 Si5
• Title of publication: A Bis(silylene)silole – Synthesis, Properties and Reactivity
• Authors of publication: Müller, Thomas; Liu, Chenghuan; Schmidtmann, Marc
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 12.3959 ± 0.0004 Å
• b: 15.5019 ± 0.0006 Å
• c: 21.2307 ± 0.0008 Å
• α: 90°
• β: 99.0856 ± 0.0012°
• γ: 90°
• Cell volume: 4028.5 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.0411
• Residual factor for significantly intense reflections: 0.0358
• Weighted residual factors for significantly intense reflections: 0.0944
• Weighted residual factors for all reflections included in the refinement: 0.0978
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No