Crystallography Open Database

Information card for entry 7716222

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Coordinates	7716222.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H106 N4 O4 Se2 Si5
Calculated formula	C68 H106 N4 O4 Se2 Si5
Title of publication	A Bis(silylene)silole – Synthesis, Properties and Reactivity
Authors of publication	Müller, Thomas; Liu, Chenghuan; Schmidtmann, Marc
Journal of publication	Dalton Transactions
Year of publication	2024
a	13.3426 ± 0.0006 Å
b	23.719 ± 0.001 Å
c	22.8201 ± 0.0009 Å
α	90°
β	98.6421 ± 0.0015°
γ	90°
Cell volume	7140 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0454
Residual factor for significantly intense reflections	0.0366
Weighted residual factors for significantly intense reflections	0.0944
Weighted residual factors for all reflections included in the refinement	0.0996
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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