Information card for entry 7716302

Structure parameters

• Formula: C40 H74 B10 N4 O0.5 P Si3
• Calculated formula: C40 H74 B10 N4 O0.5 P Si3
• Title of publication: Reactivities of phosphaalkynes towards diverse bis-silylenes.
• Authors of publication: Sun, Xiaofei; Jin, Da; Maier, Stefanie; Hinz, Alexander; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 24
• Pages of publication: 10220 - 10225
• a: 11.5007 ± 0.0017 Å
• b: 19.956 ± 0.003 Å
• c: 21.117 ± 0.003 Å
• α: 90°
• β: 94.297 ± 0.011°
• γ: 90°
• Cell volume: 4832.9 ± 1.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1517
• Residual factor for significantly intense reflections: 0.0803
• Weighted residual factors for significantly intense reflections: 0.1776
• Weighted residual factors for all reflections included in the refinement: 0.2178
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No