Information card for entry 7716442

Structure parameters

• Formula: C29 H38 B2 N12 O2 Sm
• Calculated formula: C29 H38 B2 N12 O2 Sm
• Title of publication: Activation and functionalisation of carbon dioxide by bis-tris(pyrazolyl)borate-supported divalent samarium and trivalent lanthanide silylamide complexes.
• Authors of publication: Chowdhury, Tajrian; Wilson, Claire; Farnaby, Joy H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 28
• Pages of publication: 11884 - 11894
• a: 13.9317 ± 0.0005 Å
• b: 18.7012 ± 0.0007 Å
• c: 13.5115 ± 0.0005 Å
• α: 90°
• β: 101.987 ± 0.001°
• γ: 90°
• Cell volume: 3443.5 ± 0.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0277
• Residual factor for significantly intense reflections: 0.0226
• Weighted residual factors for significantly intense reflections: 0.055
• Weighted residual factors for all reflections included in the refinement: 0.0579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No