Crystallography Open Database

Information card for entry 7716443

Preview

Coordinates	7716443.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H40 B4 N24 O4 Sm2
Calculated formula	C38 H40 B4 N24 O4 Sm2
Title of publication	Activation and functionalisation of carbon dioxide by bis-tris(pyrazolyl)borate-supported divalent samarium and trivalent lanthanide silylamide complexes
Authors of publication	Chowdhury, Tajrian; Wilson, Claire; Farnaby, Joy
Journal of publication	Dalton Transactions
Year of publication	2024
a	20.9732 ± 0.0006 Å
b	28.6287 ± 0.0008 Å
c	21.4608 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	12885.8 ± 0.6 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.0644
Residual factor for significantly intense reflections	0.0511
Weighted residual factors for significantly intense reflections	0.1389
Weighted residual factors for all reflections included in the refinement	0.1487
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.6889 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7716443.html