Information card for entry 7716445

Structure parameters

• Formula: C21 H29 B2 N12 O Si Y
• Calculated formula: C21 H29 B2 N12 O Si Y
• Title of publication: Activation and functionalisation of carbon dioxide by bis-tris(pyrazolyl)borate-supported divalent samarium and trivalent lanthanide silylamide complexes.
• Authors of publication: Chowdhury, Tajrian; Wilson, Claire; Farnaby, Joy H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 28
• Pages of publication: 11884 - 11894
• a: 19.76 ± 0.0013 Å
• b: 19.76 ± 0.0013 Å
• c: 13.3004 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4497.5 ± 0.6 ų
• Cell temperature: 273.15 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 7
• Space group number: 176
• Hermann-Mauguin space group symbol: P 63/m
• Hall space group symbol: -P 6c
• Residual factor for all reflections: 0.1456
• Residual factor for significantly intense reflections: 0.097
• Weighted residual factors for significantly intense reflections: 0.1741
• Weighted residual factors for all reflections included in the refinement: 0.1926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No