Information card for entry 7716782

Structure parameters

• Formula: C64 H490 N56 Ni55 O488 P8 Sb8 W92
• Calculated formula: C64 H240 N56 Ni55 O408 P8 Sb8 W92
• Title of publication: Two nickel-added poly(polyoxometalate)s built of Keggin-type {Ni₆PW₉} and Anderson-type NiW₆O₂₄<i>via</i> WO₄/Sb₂O bridges and Ni-O-W linkages with efficient hydrogen evolution activity.
• Authors of publication: Zhang, Peng-Yun; Lian, Chen; Wang, Zhen-Wen; Chen, Juan; Lv, Hongjin; Yang, Guo-Yu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 32
• Pages of publication: 13409 - 13415
• a: 36.8164 ± 0.001 Å
• b: 29.8064 ± 0.0008 Å
• c: 25.4292 ± 0.0007 Å
• α: 90°
• β: 105.453 ± 0.001°
• γ: 90°
• Cell volume: 26896.3 ± 1.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 8
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0638
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.0978
• Weighted residual factors for all reflections included in the refinement: 0.1024
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No