Information card for entry 8000008

Structure parameters

• Formula: C14 H56 Cl4 Co2 N6 O7 Pd S6
• Calculated formula: C14 H56 Cl4 Co2 N6 O7 Pd S6
• Title of publication: Alkylation of Nonbridging Thiolato Groups in an S-bridged CoIIIPdIICoIII Trinuclear Complex: Control of Geometrical Isomerism by Tuning Trans Influence Due to Sulfur Donors
• Authors of publication: Yu Chikamoto; Masakazu Hirotsu; Tatsuya Kawamoto; Takumi Konno
• Journal of publication: Chemistry Letters
• Year of publication: 2005
• Journal volume: 34
• Journal issue: 3
• Pages of publication: 362
• a: 16.155 ± 0.002 Å
• b: 15.088 ± 0.003 Å
• c: 17.174 ± 0.002 Å
• α: 90°
• β: 112.312 ± 0.009°
• γ: 90°
• Cell volume: 3872.8 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1803
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.1016
• Weighted residual factors for all reflections included in the refinement: 0.1555
• Goodness-of-fit parameter for all reflections included in the refinement: 0.916
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No