Information card for entry 8000009

Structure parameters

• Formula: C26 H68 Cl4 Co2 N6 O9 Pd S6
• Calculated formula: C26 H50 Cl4 Co2 N6 O9 Pd S6
• Title of publication: Alkylation of Nonbridging Thiolato Groups in an S-bridged CoIIIPdIICoIII Trinuclear Complex: Control of Geometrical Isomerism by Tuning Trans Influence Due to Sulfur Donors
• Authors of publication: Yu Chikamoto; Masakazu Hirotsu; Tatsuya Kawamoto; Takumi Konno
• Journal of publication: Chemistry Letters
• Year of publication: 2005
• Journal volume: 34
• Journal issue: 3
• Pages of publication: 362
• a: 13.024 ± 0.002 Å
• b: 16.762 ± 0.003 Å
• c: 12.618 ± 0.002 Å
• α: 111.309 ± 0.014°
• β: 98.741 ± 0.015°
• γ: 104.056 ± 0.014°
• Cell volume: 2399.8 ± 0.8 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1497
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1629
• Weighted residual factors for all reflections included in the refinement: 0.2015
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No