Information card for entry 8100877

Structure parameters

• Formula: C33 H32 B F4 O2 P2 Rh
• Calculated formula: C33 H32 B F4 O2 P2 Rh
• Title of publication: Crystal structure of 1,2-bis(diphenylphosphinoxy)-ethane rhodium(I)- norborna-2,5-diene tetrafluoroborate, C~33~H~32~BF~4~O~2~P~2~Rh, and of 1,2-bis(diphenylphosphinoxy)-ethane rhodium(I)-(Z,Z)-cycloocta- 1,5-diene tetrafluoroborate, C~34~H~36~BF~4~O~2~P~2~Rh · C~4~H~8~O · 1/4CH~2~Cl~2~
• Authors of publication: Kempe, Rhett; Spannenberg, Anke; Heller, Detlef; Kadyrov, Renat; Fehring, Volker
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2001
• Journal volume: 216
• Journal issue: 1
• Pages of publication: 157 - 160
• a: 9.342 ± 0.002 Å
• b: 10.279 ± 0.003 Å
• c: 16.964 ± 0.003 Å
• α: 74.88 ± 0.02°
• β: 82.13 ± 0.02°
• γ: 83.63 ± 0.02°
• Cell volume: 1553 ± 0.6 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.0951
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No