Crystallography Open Database

Information card for entry 1559721

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Coordinates	1559721.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H48 Cl N2 Rh Si
Calculated formula	C32 H48 Cl N2 Rh Si
Title of publication	A cyclopentadienyl functionalized silylene ‒ a flexible ligand for Si- and C-coordination
Authors of publication	Kaufmann, Sebastian; Krätschmer, Frederic; Köppe, Ralf; Schon, Thorben; Schoo, Christoph; Roesky, Peter W.
Journal of publication	Chemical Science
Year of publication	2020
Journal volume	11
Journal issue	46
Pages of publication	12446 - 12452
a	11.4019 ± 0.0006 Å
b	20.6248 ± 0.001 Å
c	13.6772 ± 0.0009 Å
α	90°
β	101.761 ± 0.005°
γ	90°
Cell volume	3148.8 ± 0.3 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0385
Residual factor for significantly intense reflections	0.0267
Weighted residual factors for significantly intense reflections	0.0675
Weighted residual factors for all reflections included in the refinement	0.0713
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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