Information card for entry 4079492

Structure parameters

• Formula: C27 H32 Ge Mo N2 O3 Si2
• Calculated formula: C27 H32 Ge Mo N2 O3 Si2
• SMILES: [Mo]1234([Ge]5[n]6ccccc6C([Si](C)(C)C)=C(N5[Si](C)(C)C)c5ccccc5)([cH]5[cH]1[cH]2[cH]3[cH]45)(C#[O])(C#[O])C#[O]
• Title of publication: Synthesis and Structural Characterization of Metallogermylenes, Cp-Substituted Germylene, and a Germanium(II)-Borane Adduct from Pyridyl-1-azaallyl Germanium(II) Chloride
• Authors of publication: Leung, Wing-Por; Chiu, Wang-Kin; Mak, Thomas C. W.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 19
• Pages of publication: 6966
• a: 14.921 ± 0.002 Å
• b: 15.088 ± 0.002 Å
• c: 26.873 ± 0.004 Å
• α: 90°
• β: 94.579 ± 0.003°
• γ: 90°
• Cell volume: 6030.6 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0422
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0774
• Weighted residual factors for all reflections included in the refinement: 0.0831
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No