Information card for entry 4321494

Structure parameters

• Formula: C62 H71 N5 O4 W
• Calculated formula: C62 H71 N5 O4 W
• Title of publication: Group 6 Metallocalixarenes Bearing "Hydrazido(2-)" Groups
• Authors of publication: Carl Redshaw; Mark R. J. Elsegood
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 5164 - 5168
• a: 10.7852 ± 0.0006 Å
• b: 14.7376 ± 0.0008 Å
• c: 18.2479 ± 0.0009 Å
• α: 94.057 ± 0.002°
• β: 91.513 ± 0.002°
• γ: 108.029 ± 0.002°
• Cell volume: 2747.6 ± 0.3 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0256
• Residual factor for significantly intense reflections: 0.0227
• Weighted residual factors for significantly intense reflections: 0.0554
• Weighted residual factors for all reflections included in the refinement: 0.0576
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No