Information card for entry 1100218

Structure parameters

• Chemical name: tetrakis(Diphenyl(methyl)phosphine)-nickel(0)
• Formula: C52 H52 Ni P4
• Calculated formula: C52 H52 Ni P4
• Title of publication: Phosphaniminato- und Phosphanimin-Komplexe von Nickel(II). Die Kristallstrukturen von [Ni(O~3~SCF~3~)(NPMe~3~)]~4~, [Ni~4~Br~5~{NP(NMe~2~)~3~}~3~], [NiBr~2~{HNP(NMe~2~)~3~}~2~] und [Ni(PMePh~2~)~4~]
• Authors of publication: Krieger, Matthias; Gould, Robert O.; Harms, Klaus; Greiner, Andreas; Dehnicke, Kurt
• Journal of publication: Zeitschrift fuer Anorganische und Allgemeine Chemie
• Year of publication: 2001
• Journal volume: 627
• Journal issue: 4
• Pages of publication: 747 - 754
• a: 10.531 ± 0.002 Å
• b: 13.15 ± 0.003 Å
• c: 16.745 ± 0.003 Å
• α: 81.547 ± 0.013°
• β: 79.148 ± 0.016°
• γ: 84.912 ± 0.018°
• Cell volume: 2248.24 ų
• Ambient diffraction temperature: 223 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 4.97
• Weighted residual factors for significantly intense reflections: 4.97
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No