Crystallography Open Database

Information card for entry 4066486

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Coordinates	4066486.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C79 H100 Ge2
Calculated formula	C79 H100 Ge2
Title of publication	Synthesis and Structures of Low-Valent Alkynyl Tin and Germanium Complexes Supported by Terphenyl Ligands: Heavier Group 14 Element Enediyne Analogues†
Authors of publication	Lei, Hao; Fettinger, James C.; Power, Philip P.
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	21
Pages of publication	5585
a	12.9836 ± 0.0008 Å
b	12.9845 ± 0.0008 Å
c	13.0755 ± 0.0008 Å
α	64.2466 ± 0.0007°
β	62.1458 ± 0.0007°
γ	65.121 ± 0.0007°
Cell volume	1688.49 ± 0.18 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0336
Residual factor for significantly intense reflections	0.0283
Weighted residual factors for significantly intense reflections	0.0722
Weighted residual factors for all reflections included in the refinement	0.0747
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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