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Information card for entry 4080890
Preview
Coordinates | 4080890.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | Ti(O(CH2CH2NSiMe3)(CH2CH2NCN(Xyl)(SiMe3))(NCNXyl)(NPh2) |
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Formula | C40 H54 N6 O Si2 Ti |
Calculated formula | C40 H54 N6 O Si2 Ti |
SMILES | [Ti]12(N=C=Nc3c(cccc3C)C)(N(c3ccccc3)c3ccccc3)N([Si](C)(C)C)CCOCC[N]1=C2N([Si](C)(C)C)c1c(cccc1C)C |
Title of publication | Synthesis and Reactivity of Titanium Hydrazido Complexes Supported by Diamido-Ether Ligands |
Authors of publication | Unruangsri, Junjuda; Morgan, Hannah; Schwarz, Andrew D.; Schofield, A. Daniel; Mountford, Philip |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 10 |
Pages of publication | 3091 |
a | 13.941 ± 0.003 Å |
b | 15.331 ± 0.003 Å |
c | 19.787 ± 0.004 Å |
α | 90° |
β | 107.51 ± 0.03° |
γ | 90° |
Cell volume | 4033.1 ± 1.6 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1122 |
Residual factor for significantly intense reflections | 0.0687 |
Weighted residual factors for all reflections | 0.0762 |
Weighted residual factors for significantly intense reflections | 0.0616 |
Weighted residual factors for all reflections included in the refinement | 0.059 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.0621 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4080890.html
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