Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4084050
Preview
Coordinates | 4084050.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C62 H109 Cl3 N2 P4 Ru2 |
---|---|
Calculated formula | C62 H108 Cl3 N2 P4 Ru2 |
SMILES | [Ru]123([Cl][Ru]4([Cl]1)([Cl]2)[P](C1CCCCC1)(C1CCCCC1)CCCC[P]4(C1CCCCC1)C1CCCCC1)([N]#N)[P](C1CCCCC1)(C1CCCCC1)CCCC[P]3(C1CCCCC1)C1CCCCC1.c1ccccc1 |
Title of publication | A Stable Silylene in a Reactive Environment: Synthesis, Reactivity, and Silicon Extrusion Chemistry of a Coordinatively Unsaturated Ruthenium Silylene Complex Containing Chloride and η3-P‒C‒P Ligands |
Authors of publication | Amoroso, Dino; Haaf, Michael; Yap, Glenn P. A.; West, Robert; Fogg, Deryn E. |
Journal of publication | Organometallics |
Year of publication | 2002 |
Journal volume | 21 |
Journal issue | 3 |
Pages of publication | 534 - 540 |
a | 11.622 ± 0.0009 Å |
b | 13.5699 ± 0.001 Å |
c | 22.7781 ± 0.0017 Å |
α | 89.723 ± 0.001° |
β | 86.837 ± 0.001° |
γ | 66.508 ± 0.001° |
Cell volume | 3289 ± 0.4 Å3 |
Cell temperature | 203 ± 2 K |
Ambient diffraction temperature | 203 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0971 |
Residual factor for significantly intense reflections | 0.0487 |
Weighted residual factors for significantly intense reflections | 0.0964 |
Weighted residual factors for all reflections included in the refinement | 0.1059 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4084050.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.