Information card for entry 4084421

Structure parameters

• Common name: Compound6
• Formula: C41 H50 N Ni P2 Si
• Calculated formula: C41 H50 N Ni P2 Si
• SMILES: c1(c(cccc1C(C)C)C(C)C)N([Si](C)(C)C)[Ni]1[P](c2ccccc2)(c2ccccc2)CC[P]1(c1ccccc1)c1ccccc1
• Title of publication: Useful Method for the Preparation of Low-Coordinate Nickel(I) Complexes via Transformations of the Ni(I) Bis(amido) Complex K{Ni[N(SiMe3)(2,6- (i) Pr2-C6H3)]2}
• Authors of publication: Lipschutz, Michael I.; Tilley, T. Don
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5566 - 5570
• a: 10.2622 ± 0.0005 Å
• b: 10.9582 ± 0.0005 Å
• c: 18.1585 ± 0.0008 Å
• α: 95.201 ± 0.002°
• β: 102.21 ± 0.002°
• γ: 108.057 ± 0.002°
• Cell volume: 1870.53 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0551
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No