Information card for entry 4133627

Structure parameters

• Formula: C54 H67 N5 O Si2
• Calculated formula: C54 H67 N5 O Si2
• Title of publication: Silicon-Mediated Selective Homo- and Heterocoupling of Carbon Monoxide.
• Authors of publication: Wang, Yuwen; Kostenko, Arseni; Hadlington, Terrance J.; Luecke, Marcel-Philip; Yao, Shenglai; Driess, Matthias
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 1
• Pages of publication: 626 - 634
• a: 16.8495 ± 0.0004 Å
• b: 13.9048 ± 0.0003 Å
• c: 22.1044 ± 0.0005 Å
• α: 90°
• β: 106.452 ± 0.003°
• γ: 90°
• Cell volume: 4966.8 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0906
• Residual factor for significantly intense reflections: 0.0515
• Weighted residual factors for significantly intense reflections: 0.1142
• Weighted residual factors for all reflections included in the refinement: 0.1381
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No