Information card for entry 4320799

Structure parameters

• Formula: Cl6 Cs2 Os2 Re4 Se8
• Calculated formula: Cl6 Cs2 Os1.98 Re4.02 Se8
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 9.8333 ± 0.0002 Å
• b: 9.8333 ± 0.0002 Å
• c: 14.1252 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1182.83 ± 0.04 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 163
• Hermann-Mauguin space group symbol: P -3 1 c
• Hall space group symbol: -P 3 2c
• Residual factor for all reflections: 0.0709
• Residual factor for significantly intense reflections: 0.0592
• Weighted residual factors for all reflections: 0.1528
• Weighted residual factors for significantly intense reflections: 0.1457
• Goodness-of-fit parameter for all reflections: 1.233
• Goodness-of-fit parameter for significantly intense reflections: 1.34
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No