Information card for entry 4322356

Structure parameters

• Formula: C140 H158 Cl6 I2 N10 Rh2
• Calculated formula: C140 H158 Cl6 I2 N10 Rh2
• Title of publication: Synthesis, Structure, and Modeling of a Cyclic Rhodium(III) Porphyrin Dimer with an Encapsulated 4,4'-Bipyridine Ligand
• Authors of publication: Hee-Joon Kim; James E. Redman; Moshe Nakash; Neil Feeder; Simon J. Teat; Jeremy K. M. Sanders
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 5178 - 5183
• a: 15.043 ± 0.002 Å
• b: 16.146 ± 0.002 Å
• c: 16.596 ± 0.002 Å
• α: 63.73 ± 0.01°
• β: 69.64 ± 0.01°
• γ: 63.23 ± 0.01°
• Cell volume: 3171.1 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1572
• Residual factor for significantly intense reflections: 0.0934
• Weighted residual factors for significantly intense reflections: 0.2086
• Weighted residual factors for all reflections included in the refinement: 0.2384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.184
• Diffraction radiation wavelength: 0.6917 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No