Information card for entry 4324727

Structure parameters

• Chemical name: N,N'-bis(trimethylsilyl)-N'-(dimethylchlorosilyl)hydrazinomethylphenyl phosphane aluminiumtrichloride adduct
• Formula: C15 H32 Al Cl4 N2 P Si3
• Calculated formula: C15 H32 Al Cl4 N2 P Si3
• Title of publication: Lewis Acid Assisted Methyl/Chlorine Exchange in Silylated Hydrazinochlorophosphanes
• Authors of publication: Andrea Westenkirchner; Alexander Villinger; Konstantin Karaghiosoff; Ronald Wustrack; Dirk Michalik; Axel Schulz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 2691 - 2702
• a: 9.7093 ± 0.0004 Å
• b: 15.834 ± 0.0005 Å
• c: 17.582 ± 0.0006 Å
• α: 90°
• β: 100.026 ± 0.002°
• γ: 90°
• Cell volume: 2661.73 ± 0.17 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0961
• Weighted residual factors for all reflections included in the refinement: 0.1025
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No