Information card for entry 4339421

Structure parameters

• Formula: C23 H52 Co F3 N O3 P2 S Si2
• Calculated formula: C23 H52 Co F3 N O3 P2 S Si2
• Title of publication: Exploring the reactivity of four-coordinate PNPCoX with access to three-coordinate spin triplet PNPCo.
• Authors of publication: Ingleson, Michael J.; Pink, Maren; Fan, Hongjun; Caulton, Kenneth G.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 24
• Pages of publication: 10321 - 10334
• a: 11.8366 ± 0.0016 Å
• b: 16.075 ± 0.002 Å
• c: 18.212 ± 0.002 Å
• α: 90°
• β: 102.677 ± 0.003°
• γ: 90°
• Cell volume: 3380.8 ± 0.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.0991
• Weighted residual factors for all reflections included in the refinement: 0.1209
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No