Information card for entry 7003526

Structure parameters

• Formula: C48 H84 Li2 N6 O2 Si4
• Calculated formula: C48 H84 Li2 N6 O2 Si4
• Title of publication: Synthesis and structures of some new types of lithium β-diketiminates
• Authors of publication: Wei, Xue-Hong; Farwell, James D.; Hitchcock, Peter B.; Lappert, Michael F.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 8
• Pages of publication: 1073 - 1080
• a: 13.7827 ± 0.0009 Å
• b: 9.7621 ± 0.0004 Å
• c: 21.3079 ± 0.0012 Å
• α: 90°
• β: 96.894 ± 0.002°
• γ: 90°
• Cell volume: 2846.2 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0892
• Residual factor for significantly intense reflections: 0.0714
• Weighted residual factors for significantly intense reflections: 0.1885
• Weighted residual factors for all reflections included in the refinement: 0.2035
• Goodness-of-fit parameter for all reflections included in the refinement: 0.952
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No