Information card for entry 7009027

Structure parameters

• Chemical name: trans dichloro tetrakis(dimethylsulfoxide) osmium(II)
• Formula: C8 H24 Cl2 O4 Os S4
• Calculated formula: C8 H24 Cl2 O4 Os S4
• Title of publication: Unusual pathways for the reaction between [MCl2(Me2SO)4] (M = Os, Ru) and hydrazine dihydrochloride: deoxygenation of sulfoxides vs. coordination of hydrazinium
• Authors of publication: da Silva, M. Fátima C. Guedes; Pombeiro, Armando J. L.; Geremia, Silvano; Zangrando, Ennio; Calligaris, Mario; Zinchenko, Andrey V.; Kukushkin, Vadim Yu.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 8
• Pages of publication: 1363
• a: 9.0951 ± 0.0007 Å
• b: 9.0951 ± 0.0007 Å
• c: 11.1941 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 925.99 ± 0.16 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.0163
• Residual factor for significantly intense reflections: 0.0163
• Weighted residual factors for all reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.0433
• Goodness-of-fit parameter for all reflections: 1.126
• Goodness-of-fit parameter for significantly intense reflections: 1.126
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No