Information card for entry 7011455

Structure parameters

• Formula: C56.5 H46 O6.5 P4 Pt2 Rh2
• Calculated formula: C56.5 H46 O6.5 P4 Pt2 Rh2
• Title of publication: Synthesis and structural characterization of mixed-metal Pt‒Rh clusters. Assembly of tetra- and tetra-hexanuclear clusters from smaller metal fragments
• Authors of publication: Koshevoy, Igor O.; Tunik, Sergey P.; Jääskeläinen, Sirpa; Haukka, Matti; Pakkanen, Tapani A.; Podkorytov, Ivan S.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 13
• Pages of publication: 2768
• a: 13.7311 ± 0.0002 Å
• b: 29.1268 ± 0.0003 Å
• c: 13.8315 ± 0.0003 Å
• α: 90°
• β: 100.868 ± 0.001°
• γ: 90°
• Cell volume: 5432.59 ± 0.15 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.0643
• Weighted residual factors for all reflections included in the refinement: 0.0671
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No