Information card for entry 7012283

Structure parameters

• Formula: C32 H92 Al Li N16 O2 Si4
• Calculated formula: C32 H92 Al Li N16 O2 Si4
• Title of publication: Syntheses and structures of [(Me3N)3SiNHLi]4, (C4H8O)Al[NHSi(NMe2)3]3, ((Me2N)3SiNH)3Al and Li(THF)2+[((Me2N)3SiNH)4Al]–
• Authors of publication: Bradley, John S.; Cheng, Fei; Archibald, Stephen J.; Supplit, Ralf; Rovai, Riccardo; Lehmann, Christian W.; Krüger, Carl; Lefebvre, Frédéric
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 9
• Pages of publication: 1846
• a: 12.2318 ± 0.0004 Å
• b: 21.7844 ± 0.0009 Å
• c: 20.2211 ± 0.0006 Å
• α: 90°
• β: 105.313 ± 0.001°
• γ: 90°
• Cell volume: 5196.9 ± 0.3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.1083
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No