Information card for entry 7012284

Structure parameters

• Formula: C22 H65 Al N12 O Si3
• Calculated formula: C22 H65 Al N12 O Si3
• SMILES: CN(C)[Si](N[Al](N[Si](N(C)C)(N(C)C)N(C)C)(N[Si](N(C)C)(N(C)C)N(C)C)[O]1CCCC1)(N(C)C)N(C)C
• Title of publication: Syntheses and structures of [(Me3N)3SiNHLi]4, (C4H8O)Al[NHSi(NMe2)3]3, ((Me2N)3SiNH)3Al and Li(THF)2+[((Me2N)3SiNH)4Al]‒
• Authors of publication: Bradley, John S.; Cheng, Fei; Archibald, Stephen J.; Supplit, Ralf; Rovai, Riccardo; Lehmann, Christian W.; Krüger, Carl; Lefebvre, Frédéric
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 9
• Pages of publication: 1846
• a: 9.7875 ± 0.0016 Å
• b: 17.413 ± 0.002 Å
• c: 21.81 ± 0.004 Å
• α: 90°
• β: 112.536 ± 0.014°
• γ: 90°
• Cell volume: 3433.2 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2143
• Residual factor for significantly intense reflections: 0.0716
• Weighted residual factors for significantly intense reflections: 0.162
• Weighted residual factors for all reflections included in the refinement: 0.2146
• Goodness-of-fit parameter for all reflections included in the refinement: 0.775
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No