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Information card for entry 7012490
Preview
Coordinates | 7012490.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H33 Ge N3 Si2 |
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Calculated formula | C27 H33 Ge N3 Si2 |
SMILES | [Ge]12N([Si](C)(C)C)C(=Cc3[n]1c(C=C(N2[Si](C)(C)C)c1ccccc1)ccc3)c1ccccc1 |
Title of publication | Synthesis and structural characterisation of low-valent Group 14 metal complexes containing tridentate 2,6-pyridyl-bridged bis(1-azaallyl) ligands |
Authors of publication | Leung, Wing-Por; Hou, Henry L.; Cheng, Hui; Yang, Qing-Chuan; Li, Hung-Wing; Mak, Thomas C. W. |
Journal of publication | Dalton Transactions |
Year of publication | 2003 |
Journal issue | 8 |
Pages of publication | 1505 |
a | 13.8767 ± 0.0018 Å |
b | 13.7394 ± 0.0018 Å |
c | 14.587 ± 0.002 Å |
α | 90° |
β | 95.11 ± 0.003° |
γ | 90° |
Cell volume | 2770.1 ± 0.6 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0482 |
Residual factor for significantly intense reflections | 0.0305 |
Weighted residual factors for significantly intense reflections | 0.0777 |
Weighted residual factors for all reflections included in the refinement | 0.0825 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.945 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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