Information card for entry 7046908

Structure parameters

• Formula: C55 H50 B2 N12 P2 Rh2
• Calculated formula: C55 H50 B2 N12 P2 Rh2
• Title of publication: Simple generation of a dirhodium μ-carbido complex via thiocarbonyl reduction.
• Authors of publication: Barnett, Harrison J.; Burt, Liam K.; Hill, Anthony F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 29
• Pages of publication: 9570 - 9574
• a: 18.8404 ± 0.0003 Å
• b: 13.263 ± 0.0002 Å
• c: 11.703 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2924.35 ± 0.08 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0356
• Residual factor for significantly intense reflections: 0.0273
• Weighted residual factors for significantly intense reflections: 0.0498
• Weighted residual factors for all reflections included in the refinement: 0.0552
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No