Information card for entry 7048017

Structure parameters

• Formula: C32 H33 F6 N7 O6 S2 Sn
• Calculated formula: C32 H33 F6 N7 O6 S2 Sn
• Title of publication: Synthesis, characterization and mass-spectrometric analysis of [LSn(IV)F_4-x]^x+ salts [L = tris ((1-ethyl-benzoimidazol-2-yl)methyl)amine, x = 1-4].
• Authors of publication: Suter, Riccardo; Swidan, Ala'aeddeen; Zijlstra, Harmen S.; Macdonald, Charles L. B.; McIndoe, J. Scott; Burford, Neil
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 46
• Pages of publication: 16729 - 16736
• a: 24.916 ± 0.0009 Å
• b: 18.9906 ± 0.0007 Å
• c: 18.5755 ± 0.0007 Å
• α: 90°
• β: 120.133 ± 0.002°
• γ: 90°
• Cell volume: 7601.6 ± 0.5 ų
• Cell temperature: 170 K
• Ambient diffraction temperature: 169.99 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0891
• Residual factor for significantly intense reflections: 0.0696
• Weighted residual factors for significantly intense reflections: 0.1395
• Weighted residual factors for all reflections included in the refinement: 0.1567
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No