Information card for entry 7107430

Structure parameters

• Formula: C35 H53 Cl N2 Pb
• Calculated formula: C35 H53 Cl N2 Pb
• Title of publication: Contrasting reductions of group 14 metal(II) chloride complexes: synthesis of a ?-diketiminato tin(I) dimer
• Authors of publication: Sam L. Choong; Christian Schenk; Andreas Stasch; Deepak Dange; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 2504
• a: 16.5359 ± 0.0004 Å
• b: 10.6225 ± 0.0002 Å
• c: 19.5757 ± 0.0005 Å
• α: 90°
• β: 100.726 ± 0.002°
• γ: 90°
• Cell volume: 3378.45 ± 0.14 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0339
• Residual factor for significantly intense reflections: 0.0228
• Weighted residual factors for significantly intense reflections: 0.0443
• Weighted residual factors for all reflections included in the refinement: 0.0487
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No