Information card for entry 7120530
| Formula |
C102 H152 B2 K2 O18 |
| Calculated formula |
C102 H152 B2 K2 O18 |
| Title of publication |
Consecutive reduction, radical-cyclization, and oxidative-dehydrogenation reaction of ortho-substituted diboryl compound |
| Authors of publication |
Yu, Lirong; Li, Yanglizhi; Wang, Xi; Wang, Xingyong; Zhou, Panpan; Jiang, ShangDa; pan, xiaobo |
| Journal of publication |
Chem. Commun. |
| Year of publication |
2017 |
| a |
12.8138 ± 0.0005 Å |
| b |
13.8501 ± 0.0006 Å |
| c |
16.3243 ± 0.0007 Å |
| α |
104.712 ± 0.004° |
| β |
107.141 ± 0.004° |
| γ |
103.546 ± 0.004° |
| Cell volume |
2523.5 ± 0.2 Å3 |
| Cell temperature |
293 ± 2 K |
| Ambient diffraction temperature |
293 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.1337 |
| Residual factor for significantly intense reflections |
0.0894 |
| Weighted residual factors for significantly intense reflections |
0.2362 |
| Weighted residual factors for all reflections included in the refinement |
0.2779 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.045 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7120530.html
