Crystallography Open Database

Information card for entry 7124624

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Coordinates	7124624.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C57 H55 B F15 N6 Nb
Calculated formula	C57 H55 B F15 N6 Nb
Title of publication	Photo-activation of d(0) niobium imido azides: en route to nitrido complexes.
Authors of publication	Camp, Clément; Grant, Lauren N.; Bergman, Robert G.; Arnold, John
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	32
Pages of publication	5538 - 5541
a	12.2684 ± 0.0005 Å
b	12.7008 ± 0.0005 Å
c	19.2268 ± 0.0008 Å
α	79.4526 ± 0.0019°
β	83.1067 ± 0.0017°
γ	68.923 ± 0.0016°
Cell volume	2743.4 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0366
Residual factor for significantly intense reflections	0.0311
Weighted residual factors for significantly intense reflections	0.0713
Weighted residual factors for all reflections included in the refinement	0.0749
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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