Information card for entry 7130878

Structure parameters

• Formula: C26 H72 N5 Si8 Yb
• Calculated formula: C26 H72 N5 Si8 Yb
• Title of publication: Nitrile formation via dichlorocarbene insertion into the Si-N bond of Ln(III) bis(trimethylsilyl)amide complexes
• Authors of publication: Li, Yangjuan; Gong, Yu
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 20.0586 ± 0.0003 Å
• b: 20.0586 ± 0.0003 Å
• c: 23.4376 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9430.1 ± 0.3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 110
• Hermann-Mauguin space group symbol: I 41 c d
• Hall space group symbol: I 4bw -2c
• Residual factor for all reflections: 0.0308
• Residual factor for significantly intense reflections: 0.0225
• Weighted residual factors for significantly intense reflections: 0.0556
• Weighted residual factors for all reflections included in the refinement: 0.0611
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No