Information card for entry 7700999

Structure parameters

• Formula: C24 H114 Ge2 Mo24 N6 O98
• Calculated formula: C24 Ge2 Mo24 N6 O90.6
• Title of publication: A "directed precursor self-assembly" strategy for the facile synthesis of heteropoly blues: crystal structures, formation mechanism and electron distribution.
• Authors of publication: Wang, Yuchao; Li, Fengyan; Jiang, Ning; Liu, Xizheng; Xu, Lin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 38
• Pages of publication: 14347 - 14353
• a: 41.9535 ± 0.0013 Å
• b: 12.6307 ± 0.0002 Å
• c: 22.2985 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11816 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0735
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for significantly intense reflections: 0.1407
• Weighted residual factors for all reflections included in the refinement: 0.1498
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No